English to Russian Science Chemistry; Chem Sci/Eng

A slurry experiment was performed by weighing 2.5 mg of Example 1 into a vial and adding ethanol (100 µL). The slurry was shaken for 7 days at ambient temperature and then crystals were collected using a small spatula. The crystals were dried in a hood for one hour and then analyzed using DSC (differential scanning calorimetry). A sample was weighed into an aluminium pan with a pierced lid and heated from 0°C to 300°C with a ramp of 5°C/min and modulated with the amplitude of ±0.6°C every 45 seconds. The instrument was purged with nitrogen at 50mL/minute; melting point 119±5°C.